Bisphenol A (BPA) determination in mineral water by using CG/DCE – a new analysis methodology proposal
Vol. 71 No. 4 (2012), ORIGINAL ARTICLE
Vol. 71 No. 4 (2012)

Bisphenol A (BPA) determination in mineral water by using CG/DCE – a new analysis methodology proposal

ORIGINAL ARTICLE
https://doi.org/10.53393/rial.2012.71.32475
Published 2012-12-01
Marcia Helena de Rizzo da Matta
Universidade Federal de Mato Grosso do Sul, Centro de Ciências Exatas e Tecnologias, Campo Grande, MS
Alecsandra Leite Pereira
Universidade Federal de Mato Grosso do Sul, Centro de Ciências Exatas e Tecnologias, Campo Grande, MS
Émerson Montagner
Universidade Federal de Mato Grosso do Sul, Centro de Ciências Exatas e Tecnologias, Campo Grande, MS
Guilherme Vilalba Fortunato
Universidade Federal de Mato Grosso do Sul, Centro de Ciências Exatas e Tecnologias, Campo Grande, MS
PDF (Português (Brasil))

Keywords

bisphenol A
mineral water
GC/ECD

How to Cite

1.
Matta MH de R da, Pereira AL, Montagner Émerson, Fortunato GV. Bisphenol A (BPA) determination in mineral water by using CG/DCE – a new analysis methodology proposal. Rev Inst Adolfo Lutz [Internet]. 2012 Dec. 1 [cited 2024 Jul. 22];71(4):624-9. Available from: https://periodicos.saude.sp.gov.br/RIAL/article/view/32475
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Abstract

This study evaluated the methodology for determining bisphenol A (BPA) in mineral water by using the solid phase extraction (SPE), the derivatization with trifluoroacetic anhydride (TFAA), and the gas chromatography with electron capture detector (GC/ECD) analysis. The analytical curve provided the correlation coefficient (R) of 0.999, and the recovery values from 88 to 106%. The limit of detention was 2.5 and the limit of quantification was 25.0 ng.mL-1. Four mineral water samples from different brands were analyzed by this methodology and among them only one (sample 3) showed detectable result of 0.46 ng.mL-1. This study suggested that BPA could be easily detected and quantified in mineral water samples by employing the proposed methodology, which was selective, accurate and precise.
https://doi.org/10.53393/rial.2012.71.32475
PDF (Português (Brasil))

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