Determinação espectrofotométrica de ciclamato de sódio em alimentos e bebidas dietéticas e de baixas calorias

Mônica C. R. de Camargo; Maria Cecília F. Toledo

doi:10.53393/rial.2006.65.32880

Vol. 65 No. 2 (2006), ORIGINAL ARTICLE

Vol. 65 No. 2 (2006)

Sodium cyclamate determination in dietetics and low calories foods and beverages by spectrophotometry

ORIGINAL ARTICLE

https://doi.org/10.53393/rial.2006.65.32880

Published 2006-04-01

Mônica C. R. de Camargo⁺⁻
Maria Cecília F. Toledo⁺⁻

Mônica C. R. de Camargo

Universidade Estadual de Campinas, Faculdade de Engenharia de Alimentos, Campinas, SP

Maria Cecília F. Toledo

Universidade Estadual de Campinas, Faculdade de Engenharia de Alimentos, Campinas, SP

PDF (Português (Brasil))

Keywords

intense sweeteners
sodium cyclamate
food analysis
low calorie products

How to Cite

1.

Camargo MCR de, Toledo MCF. Sodium cyclamate determination in dietetics and low calories foods and beverages by spectrophotometry. Rev Inst Adolfo Lutz [Internet]. 2006 Apr. 1 [cited 2024 Jul. 22];65(2):100-5. Available from: https://periodicos.saude.sp.gov.br/RIAL/article/view/32880

Abstract

The present study was conducted in order to determine sodium cyclamate concentrations in tabletop sweeteners, powdered sweeteners, diet/light soft drinks, diet/light teas, light yogurts, light nectars and dried mixture for light beverages, available in markets of Campinas city. Determination of this sweetener product was performed by ultraviolet spectrophotometry. Sodium cyclamate was quantitatively converted to N,N-dichlorocyclohexylamine, which was determined by measuring its UV absorption at 314 nm. Cyclamate concentration varied according to the analyzed matrix in a range from 64.9 to 95.0 mg/mL in tabletop sweeteners, 79.0 to 94.4 mg/g in powdered sweeteners, 36.1 to 101.1 mg/100mL in diet/light soft drinks, 22.7 to 54.0 mg/100mL in diet/light teas, 8.36 to 105.0 mg/100mL in light nectars, and 83.6 to 122.5 mg/100mL in light yogurts. The unique brand of mixture for beverages available, the mean quantity of this sweetener was 28.2 mg/100 mL. In general, sodium cyclamate concentration in the analyzed samples did not exceed the maximum limit established by the Brazilian Legislation.

https://doi.org/10.53393/rial.2006.65.32880

PDF (Português (Brasil))

References

1. Henin N. Intake of sweeteners, physiological and nutritional aspects. Int Sugar J. 2001; 103: 346-51.

2. Toledo MCF. Aditivos Alimentares. In: Oga S, editor. Fundamentosde Toxicologia. São Paulo: Ed Atheneu; 1996. p.405-39.

3. Bopp BA, Price P. Cyclamate. In: Nabors LOB, editor. AlternativeSweeteners 3rd ed. New York: Marcel Dekker Inc.; 2001. p.63-85.

4. Miller WT. The legacy of cyclamate. Food Technol. 1987; 41:116.

5. Brasil. Resolução de Diretoria Colegiada (RDC) nº 3, de 2 de jan.2001 da Secretaria de Vigilância Sanitária do Ministério da Saúde. Diário Oficial [da] República Federativa do Brasil, Brasília, Poder Executivo, DF, 3 jan 2001.

6. Brasil. Resolução de Diretoria Colegiada (RDC) no 271, de 22 de set. 2005 da Secretaria de Vigilância Sanitária do Ministério da Saúde. Diário Oficial [da] República Federativa do Brasil, Poder Executivo, Brasília, DF, 23 set. 2005.

7. Sjöberg AMK, Alanko TA. Spectrophotometric determination of cyclamate in foods: Nordic Committee on Food Analysis Collaborative Study. J Assoc Off Ana Chem, 1987; 70: 588-90.

8. Miller JC, Miller JN. Statistics for Analytical Chemistry. 3rd ed. Chicago(IL): Ellis Horwood Limited Publishers; 1993. p. 101-39.

9. Horwitz W, Laverne RK; Boyer KW. Quality Assurance in the analysesof foods for trace constituents. J Assoc Anal Chem, 1980; 636: 1344-54, 1980.

This work is licensed under a Creative Commons Attribution 4.0 International License.

Downloads

Download data is not yet available.