Keywords
B-asarone in alcoholic beverages, determination
flavor (calamus oil ) in alcoholic beverages
calamus oil in alcoholic beverages
alcoholic beverages, flavor
oil, calamus, in alcoholic beverages
flavor (calamus oil ) in alcoholic beverages
calamus oil in alcoholic beverages
alcoholic beverages, flavor
oil, calamus, in alcoholic beverages
How to Cite
1.
Yabiku HY, Lajolo FM. Determination of β-asarone in alcoholic beverages. Rev Inst Adolfo Lutz [Internet]. 1980 Dec. 30 [cited 2024 May 14];40(2):135-4. Available from: https://periodicos.saude.sp.gov.br/RIAL/article/view/36980
Abstract
In order to evalu a te the presence of calamus oil in alco ho lic beverages, a qua n ti ta tive de tcrminati on of i ts active principIe f3-asarone was p er Io rmed, by means of two diffcren t methods: fl uo rome t r ic and gas liquid ch roma tograph y, and accomplished with a tomic mass spect rophotcme tric a nalysis. In 56 sarriples of alcoh ol ic beverages of 18 different brands, only one demonstrated to be in higher coritcn t tha n th e permittcd limit of 1 ppm, de tc rmi ned by Europe Counci!. The f3-asarone contents varied from O ~o 4.96 p pm. It was suggested to employ the gas liquid chromatography technique as official method for determination of f3-asarone in alcoholic beverages, since it is more specif ic than fluo r ime tr ic me tho d.
References
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15. LARRY, D. - Gas-Iiquid chromatographic determination of ,8-nsarone a component of oil of calamus, in flavors and beverages. J. Assoc. off. agric. Chem., 56: 1281-3, 1973.
16. LIDDLE, P.A.P. & SMEDT, P. - Détection et dosage de quatre composés limites par diverses législations dans les boissons alcooliques. Ann. Falei], Expert, Cliim., 69 :857-64, 1976.
17. MADAN, B.R.; ARORA, R.B. & KANTl KAPlLA, M.B. - An ticonvulsan t, a n tiveratrinio and antiarrhythmic actions of AcoJ'us calarnus Linn. An Indian indigenous drug. Areh. int. Pharmacodun, Thér., 124:201-11, 1960.
18. MERAT, E.; MARTlN, E.; DURET, M. & VOGEL, J. - Extraction and gas chromatographic determination of ,8-asarone and a - f3 - thujone in aperitifs. Mit.t, Geb. -Lebens mit.t elusiiere, Hyg., 67 (4) : 521-6, 1976 apud Chem. Abstr., 86:153870j, 1977.
19. TAYLOR, J.M.; JONES, W.I.; HAGAN, E.C.; GROSS, M.A.; DAVlS, D.A. & COOK, E.L. - Toxicity of oil of calarnus (Jammu variety). Toxicol. appl. Pharmacol., 10: 405, 1967. [Abstr. 72!.
20. WOJTOWICZ, E.J. Spectrofluorometric determination of ,8-asarone in sweet and dry verrnouths. J. agric, Food Ch em., 2-1: 526-8, 1976.
2. BRASIL. Leis, decretos, etc, - Decreto nº 55.871 de 26 de março de 1965. Diário Oficial, Brasília, 9 abro 1965. Seção 1, pt. 1, p. 3610. Modifica o Decreto nº 50.040 de 24 de janeiro de 1961, referente a normas reguladoras do emprego de aditivos para alimentos, alterado pelo Decreto nº 691, de 13 de março de 1962.
3. CA VAZZA, G. - Les chímtctypcs parmi les plantes aroma tiques cas du calamus po lyploide. Ann. Falsif. Expert. chim., 69: 81;3-44, 1976.
4 CHOPRA, r.c.. JAMWAL, K.S. & KHAJURIA, B.N. - Pharmacological action of some common essential oil-bearing plan ts used in indigenous medicine. Part I. Pharmacolcgical action of Aco,.l1s calamus, CVl'e1i11",a zedoal'ia, Xo.nth.oxulu-m alai.urn
and Angelica a.rch aruielica, lndian J. medo Res., 42 :381-4, 1954.
5. CODE of Federa\ Regulations. 21. Food and lh·ui)'s. Wash ing to n , D.e., Govt. print. off., 1977. Parts 100 to 199, p. 649, paragr. 189.110.
6. COUNCIL OF EUROPE - Natural flavouring substanees, their sources, and added art.ijicial. flavouring substances. Strasbourg, 1974. p. 34.
7. DANDIYA, P.C.; BAXTER, R.M. & CULLUMBINE, H. - Studies on Acor/ls cala; mUB (I) - "Phytochemical investigation". Cano pharm, J., 91: 63-607 - 63-610, 1958.
8. DANDIYA, P.C.; BAXTER, R.M.; WALKER, G.C. & CULLUMBlNE, H. - Studies on .4.C01'l1Scalamice, par t Ir: investigation of vola+ile oi!. J. Phu rm, Ph.armacol., 11: 163-8, 1959.
9, DANDIYA, P.C. & eULLUMBINE, H. Studies on Aeoms calarmis (Tl l ) : some pharrnacological actions of the volatile oi!. J. Pluirmacol, e.cp : Ther., 125 :353-9, 1959.
10. DYER, R.H.; MARTlN, G.E. & BUSCEMl, P.C. - Gas-Iiquid chromatographic determination of f3-asarone in wines and flavors. J. Assoc. off. agric. Chem., 59 :675-7, 1976.
11. FOSTER D. SNELL, INC. - A reuort on 90-day calamus feeding etiulies icith. the hydroalcoholic ext.ract oi Acorus calamus europeati variet u, New Jersey, 1969.
12. FOSTER D. SNELL, INC. - Supplementary repo rt liuer lesions project 10002-001. New Jersey, 1969.
13. GROSS, M.A.; JONES, W.L; COOK, E.L. & BOONE, e.c. - Carcinogenici ty of oil of calamus, Proc, amo Assoc. Ctincer Res., 8:24, 1967. [Abstr. 931.
14. GUENTHER, E. - The eeeeniial oils, New York, Van Nostrand, 1952. v. 6, p. 109-17.
15. LARRY, D. - Gas-Iiquid chromatographic determination of ,8-nsarone a component of oil of calamus, in flavors and beverages. J. Assoc. off. agric. Chem., 56: 1281-3, 1973.
16. LIDDLE, P.A.P. & SMEDT, P. - Détection et dosage de quatre composés limites par diverses législations dans les boissons alcooliques. Ann. Falei], Expert, Cliim., 69 :857-64, 1976.
17. MADAN, B.R.; ARORA, R.B. & KANTl KAPlLA, M.B. - An ticonvulsan t, a n tiveratrinio and antiarrhythmic actions of AcoJ'us calarnus Linn. An Indian indigenous drug. Areh. int. Pharmacodun, Thér., 124:201-11, 1960.
18. MERAT, E.; MARTlN, E.; DURET, M. & VOGEL, J. - Extraction and gas chromatographic determination of ,8-asarone and a - f3 - thujone in aperitifs. Mit.t, Geb. -Lebens mit.t elusiiere, Hyg., 67 (4) : 521-6, 1976 apud Chem. Abstr., 86:153870j, 1977.
19. TAYLOR, J.M.; JONES, W.I.; HAGAN, E.C.; GROSS, M.A.; DAVlS, D.A. & COOK, E.L. - Toxicity of oil of calarnus (Jammu variety). Toxicol. appl. Pharmacol., 10: 405, 1967. [Abstr. 72!.
20. WOJTOWICZ, E.J. Spectrofluorometric determination of ,8-asarone in sweet and dry verrnouths. J. agric, Food Ch em., 2-1: 526-8, 1976.
This work is licensed under a Creative Commons Attribution 4.0 International License.
Copyright (c) 1980 Instituto Adolfo Lutz Journal
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