Comparative study of the usual methods for the determination of arsenic
pdf (Português (Brasil))

Keywords

arsenic in food additives, determination
food additives, arsenic determination in
methods, comparative study

How to Cite

1.
Yabiku HY, Dias NA, Martins MS. Comparative study of the usual methods for the determination of arsenic. Rev Inst Adolfo Lutz [Internet]. 1989 Jun. 30 [cited 2024 May 20];49(1):51-5. Available from: https://periodicos.saude.sp.gov.br/RIAL/article/view/36931

Abstract

In order to select the best method for determination of arsenic in food additives, the authors carried a comparative study of the three following methods; Gutzeit, colorimetric procedure of molybdenum blue and the silver diethyldithiocarbamate. The results showed that the Gutzeit method is the least sensitivo, so far, utilizing in semi-quantitative determinations. The larger coefficients of variation for silver diethyldithiocarbamate and molybdenum blue methods were obtained in low levels of arsenic determination. These methods are applica-
ble over a much wider range of arsenic contents. Silver diethyldithiocarbamate method is better for determination of low arsenic levels and molybdenum blue for high levels.

https://doi.org/10.53393/rial.1989.49.36931
pdf (Português (Brasil))

References

1. ASSOCIATION OF OFFICIAL ANALYTICAL CHEMISTS - Official methods of analysis of the Association of Official Analytical Chemists. 13th ed. Washington, D.C., A.O.A.C., 1980. p. 386 (25.010;25011)

2. ESTADOS UNIDOS. National Academy of Sciences. Food and Nutrition Board - Food chemicals codex. 3rded. Washington, D.C., National Acadenic Press, 1981. p. 464-6.

3. HOFFMAN, I. & GORDON, A.D. - Arsenic in foods: collaborative comparison of the arsine-rnolybdenum blue and the silver dicthyldithiocarbamate methods. J. Assc. off. anal. Chem., 46 (2):245-9,1963.

4. JOINT FAO/WHO EXPERT COMMITTEE ON FOOD ADDITIVES, Geneva, 1984-Specificationsfor identity and purity of certainfood additives. Rome, FAO, 1984. p. 17-22 (FAO Food and Nutrition Paper 3112)

5. SÃO PAULO. Instituto Adolfo Lutz - Normas analiticas do Instituto Adolfo Lutz. v. I: métodos químicos e físicos para análise de alimentos. 3ª ed. São Paulo, 1985. p. 67-70.

6. SAX, N.I. -Dangerous properties of industrial materials. 5thed. NewYork, VanNostrand/Reinhold, 1979. p. 388-90.
Creative Commons License

This work is licensed under a Creative Commons Attribution 4.0 International License.

Copyright (c) 1989 Instituto Adolfo Lutz Journal

Downloads

Download data is not yet available.